Cyclohexene epoxidation with H<sub>2</sub>O<sub>2</sub>in the vapor and liquid phases over a vanadium-based metal-organic framework
  • Yoon, Tae-Ung
  • Ahn, Sol
  • Kim, Ah-Reum
  • Notestein, Justin M.
  • Farha, Omar K.
  • 외 1명
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초록

A metal-organic framework, MIL-47(V) containing coordinatively saturated V(+IV)sites linked together by terephthalic linkers, was prepared by a solvothermal method and evaluated as a catalyst in the epoxidation of cyclohexene. We have compared the catalytic activity in the condensed and gas phase oxidation of cyclohexene to discuss the effect of temperature and reaction phase in cyclohexene epoxidation over MIL-47(V). The catalysts were examined for the epoxidation of cyclohexene with H(2)O(2)at 50, 65, 120, and 150 degrees C. We observed significant differences in product selectivity between liquid-phase and gas-phase operations and confirmed that the active sites are tightly incorporated into the MOF as node channels and thus resistant to leaching.

키워드

HYDROGEN-PEROXIDEOXIDATIONCATALYSTSOXIDEZEOLITESH2O2TI
제목
Cyclohexene epoxidation with H<sub>2</sub>O<sub>2</sub>in the vapor and liquid phases over a vanadium-based metal-organic framework
저자
Yoon, Tae-UngAhn, SolKim, Ah-ReumNotestein, Justin M.Farha, Omar K.Bae, Youn-Sang
DOI
10.1039/d0cy00833h
발행일
2020-07
유형
Article
저널명
Catalysis Science and Technology
10
14
페이지
4580 ~ 4585